September 10, 2025Journal of Neonatal SurgeryOpen Access

Analytical Method Development and Validation of RP-HPLC Method for Estimation of Linagliptin in Bulk and Pharmaceutical Dosage Form

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Analytical method validates accurate linagliptin measurement in pharmaceutical dosage form, suggesting robust application.

The RP-HPLC method demonstrated an accuracy of 99.7%, and complied with system suitability standards.
Linearity for linagliptin was established between 10–30 μg/mL, with a correlation coefficient of r² = 0.999.
The method utilized a Zorbax SB Phenyl column with a retention time of 2.73 minutes at 295 nm detection.
Analyzing linagliptin in pharmaceutical dosage forms was successfully conducted, ensuring reliable and precise results.

Khaladkar et al. (2025) studied this question.

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