Cascade Hydrothiolation and Hydroamidation of Alkynes to Regioselectively Afford 1,2‐Disubstituted Alkane Derivatives under Photocatalysis

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The reaction produces 1,2-disubstituted alkanes under mild conditions, showcasing the efficacy of the method.
Central to the method is hydrogen atom transfer, which facilitates selective activation during the process.
This approach utilizes visible-light photocatalysis, representing an alternative strategy for alkene functionalization.
The findings suggest broader implications for obtaining diheteroatom-substituted alkanes in organic synthesis.

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Visible-light-mediated hydrofunctionalization improves product selectivity in alkynes, indicating new synthetic pathways.

Fu et al. (2025) studied this question.

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