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September 12, 2025Journal of Separation ScienceOpen Access

Enhanced Energized Dispersive–Guided Extraction Using Doehlert Matrix Optimization and Antioxidant Evaluation of Phenolic Compounds From Herbal Leaves by Using High‐Performance Liquid Chromatography

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Authors

RSRosianne P. SilvaPSPaulo Natan Alves dos SantosLNLuciana Lordêlo Nascimento

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Overview

This research optimizes extraction using Doehlert matrix and evaluates antioxidant capacity in hydroethanolic extracts, suggesting synergistic effects among phenolic compounds.

Key Points

  • The optimized method significantly improved the yield of phenolic compounds and antioxidant properties.
  • Optimal conditions included 40% ethanol and 60% water at 165.82°C for 6.03 minutes, achieving a total phenolic content of 69.18 mg GAE/g.
  • High-performance liquid chromatography was used to reveal phenolic acids, including rutin and theophylline, enhancing the understanding of herbal constituents.
  • Correlation analysis indicated potential synergistic interactions among the active compounds found in the extracts.

Cite This Study

Silva et al. (2025) studied this question.

synapsesocial.com/papers/68d41d9b713b0b5dfea667c3https://doi.org/10.1002/jssc.70250
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